Alkylresorcinols in rye (Secale cereale L.) grains. I. Micromethod for determination of alkyl derivatives of resorcinol in rye grain

W. Mejbaum-Katzenellenbogen, F. Tłuścik, A. Kozubek, A. Sikorski

Abstract


A pure preparation of alkylresorcinol from rye grains was obtained by preparative thin-layer chromatography, which gave a UV spectrum characteristic for 5-n-alkylresorcinols and orcinol. This preparation served as standard in the elaboration of a micro method (for alkylresorcinols determination in acetone extract from rye grain. It was found that this method is suitable for selective determination of 5-n-alkylrezorcinols in acetone extracts from rye grains.

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DOI: https://doi.org/10.5586/asbp.1975.044

Journal ISSN:
  • 2083-9480 (online)
  • 0001-6977 (print; ceased since 2016)
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Polish Botanical Society